Fabrication and characterization of LRE1+xBa2-xCu3Oy (LRE

Nd, Eu, Gd, NEG) superconductors: A low oxygen partial pressure

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4 Citations (Scopus)

Abstract

We studied the effect of oxygen partial pressure reduction to 0.05% during melt processing of NdBa2Cu3Oy, EuBa2Cu3Oy, GdBa2Cu3Oy, and (Nd,Eu,Gd)Ba2Cu3Oy on magnetic properties and microstructure. The superconducting transition of all the optimally oxygenated samples was as narrow as in those prepared in pO2 of 0.1%, the onset temperature of the present samples was slightly higher or at least same as for 0.1% pO2. Optical and scanning electron microscopy showed that in the GdBa2Cu3Oy and EuBa2Cu3Oy clusters are formed of sub-micron sized secondary phase particles. In other two compounds the secondary phase was uniformly dispersed. Magnetic properties of the present samples were always better at low fields than those of the samples prepared in 0.1% pO2. The irreversibility field data were rather controversial, in some samples improved, in others worse.

Original languageEnglish
Pages (from-to)646-650
Number of pages5
JournalPhysica C: Superconductivity and its Applications
Volume378-381
Issue numberPART 1
DOIs
Publication statusPublished - 2002 Oct 1
Externally publishedYes

Fingerprint

Partial pressure
Superconducting materials
partial pressure
Magnetic properties
Oxygen
Fabrication
fabrication
oxygen
Microstructure
Scanning electron microscopy
magnetic properties
Processing
pressure reduction
Temperature
microstructure
scanning electron microscopy
temperature

Keywords

  • Critical current density (J)
  • Flux pinning
  • LRE-BaCuO
  • Melt processing
  • Microstructure

ASJC Scopus subject areas

  • Condensed Matter Physics

Cite this

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title = "Fabrication and characterization of LRE1+xBa2-xCu3Oy (LRE: Nd, Eu, Gd, NEG) superconductors: A low oxygen partial pressure",
abstract = "We studied the effect of oxygen partial pressure reduction to 0.05{\%} during melt processing of NdBa2Cu3Oy, EuBa2Cu3Oy, GdBa2Cu3Oy, and (Nd,Eu,Gd)Ba2Cu3Oy on magnetic properties and microstructure. The superconducting transition of all the optimally oxygenated samples was as narrow as in those prepared in pO2 of 0.1{\%}, the onset temperature of the present samples was slightly higher or at least same as for 0.1{\%} pO2. Optical and scanning electron microscopy showed that in the GdBa2Cu3Oy and EuBa2Cu3Oy clusters are formed of sub-micron sized secondary phase particles. In other two compounds the secondary phase was uniformly dispersed. Magnetic properties of the present samples were always better at low fields than those of the samples prepared in 0.1{\%} pO2. The irreversibility field data were rather controversial, in some samples improved, in others worse.",
keywords = "Critical current density (J), Flux pinning, LRE-BaCuO, Melt processing, Microstructure",
author = "Muralidhar Miryala and Naomichi Sakai and M. Jirsa and Masato Murakami",
year = "2002",
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T2 - Nd, Eu, Gd, NEG) superconductors: A low oxygen partial pressure

AU - Miryala, Muralidhar

AU - Sakai, Naomichi

AU - Jirsa, M.

AU - Murakami, Masato

PY - 2002/10/1

Y1 - 2002/10/1

N2 - We studied the effect of oxygen partial pressure reduction to 0.05% during melt processing of NdBa2Cu3Oy, EuBa2Cu3Oy, GdBa2Cu3Oy, and (Nd,Eu,Gd)Ba2Cu3Oy on magnetic properties and microstructure. The superconducting transition of all the optimally oxygenated samples was as narrow as in those prepared in pO2 of 0.1%, the onset temperature of the present samples was slightly higher or at least same as for 0.1% pO2. Optical and scanning electron microscopy showed that in the GdBa2Cu3Oy and EuBa2Cu3Oy clusters are formed of sub-micron sized secondary phase particles. In other two compounds the secondary phase was uniformly dispersed. Magnetic properties of the present samples were always better at low fields than those of the samples prepared in 0.1% pO2. The irreversibility field data were rather controversial, in some samples improved, in others worse.

AB - We studied the effect of oxygen partial pressure reduction to 0.05% during melt processing of NdBa2Cu3Oy, EuBa2Cu3Oy, GdBa2Cu3Oy, and (Nd,Eu,Gd)Ba2Cu3Oy on magnetic properties and microstructure. The superconducting transition of all the optimally oxygenated samples was as narrow as in those prepared in pO2 of 0.1%, the onset temperature of the present samples was slightly higher or at least same as for 0.1% pO2. Optical and scanning electron microscopy showed that in the GdBa2Cu3Oy and EuBa2Cu3Oy clusters are formed of sub-micron sized secondary phase particles. In other two compounds the secondary phase was uniformly dispersed. Magnetic properties of the present samples were always better at low fields than those of the samples prepared in 0.1% pO2. The irreversibility field data were rather controversial, in some samples improved, in others worse.

KW - Critical current density (J)

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KW - LRE-BaCuO

KW - Melt processing

KW - Microstructure

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