Magnetic phases in superconducting, polycrystalline bulk FeSe samples

Quentin Nouailhetas, Anjela Koblischka-Veneva, Michael R. Koblischka, Pavan Kumar S. Naik, Florian Schäfer, H. Ogino, Christian Motz, Kévin Berger, Bruno Douine, Yassine Slimani, Essia Hannachi

Research output: Contribution to journalArticlepeer-review

Abstract

The FeSe compound is the simplest high-temperature superconductor (HTSc) possible, and relatively cheap, not containing any rare-earth material. Although the transition temperature, Tc, is just below 10 K, the upper critical fields are comparable with other HTSc. Preparing FeSe using solid-state sintering yields samples exhibiting strong ferromagnetic hysteresis loops (MHLs), and the superconducting contribution is only visible after subtracting MHLs from above Tc. Due to the complicated phase diagram, the samples are a mixture of several phases, the superconducting β-FeSe, and the non-superconducting δ-FeSe and γ-FeSe. Furthermore, antiferromagnetic Fe7Se8 and ferromagnetic α-Fe may be contained, depending directly on the Se loss during the sintering process. Here, we show MHLs measured up to ±7 T and determine the magnetic characteristics, together with the amount of superconductivity determined from M(T) measurements. We also performed a thorough analysis of the microstructures in order to establish a relation between microstructure and the resulting sample properties.

Original languageEnglish
Article number015230
JournalAIP Advances
Volume11
Issue number1
DOIs
Publication statusPublished - 2021 Jan 1

ASJC Scopus subject areas

  • Physics and Astronomy(all)

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