Microstructural characteristics of melt-powder-melt-grown YBa2Cu3O7-x crystals

R. Miletich, Masato Murakami, A. Preisinger, H. W. Weber

Research output: Contribution to journalArticle

16 Citations (Scopus)

Abstract

Melt-powder-melt-grown crystals of high-Tc YBa2Cu3O7-δ were prepared from different chemical starting compositions. They all show well textured microstructures with characteristic differences and various amounts of included phases (Y2BaCuO5, Ba4Cu2PtO9, and metallic silver) depending on the starting composition. Detailed investigations with polarized reflected light, XRF, EDX and X-ray diffraction reveal characteristic features of the microstructure such as the distribution of included phases as well as twinning and crack formation, which are related to local variations in oxygen content in these materials. Increasing silver contents result in a reduction of cracking. The occurence of domain-like regions with distinct large twin lamellae is correlated with the distribution of Y2BaCuO5 inclusions.

Original languageEnglish
Pages (from-to)415-420
Number of pages6
JournalPhysica C: Superconductivity and its Applications
Volume209
Issue number4
DOIs
Publication statusPublished - 1993 May 1
Externally publishedYes

Fingerprint

Silver
Powders
silver
Crystals
microstructure
Microstructure
crack initiation
Twinning
lamella
Light polarization
twinning
Chemical analysis
Crack initiation
crystals
Energy dispersive spectroscopy
inclusions
Oxygen
X ray diffraction
oxygen
diffraction

ASJC Scopus subject areas

  • Condensed Matter Physics

Cite this

Microstructural characteristics of melt-powder-melt-grown YBa2Cu3O7-x crystals. / Miletich, R.; Murakami, Masato; Preisinger, A.; Weber, H. W.

In: Physica C: Superconductivity and its Applications, Vol. 209, No. 4, 01.05.1993, p. 415-420.

Research output: Contribution to journalArticle

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