抄録
Here, we report the growth of magnesium diboride (MgB2) single crystals under high-pressure in the Mg-B-N system. The phase stability limit of MgB2 in P-T space was determined and reaction diagram for the crystal growth of MgB2 under high-pressure was proposed. It was found that utilization of longitudinal temperature gradient and optimisation of reactant pellets locations in the BN high-pressure cell is very helpful for reproducible growth of MgB2 single crystals of various shapes and size of 200-700 μm. The high-quality of the samples was confirmed by single crystal X-ray diffraction and sharp superconducting transitions at Tc = 38.1-38.3K obtained in both magnetization (ΔTc = 0.6 K) and resistivity (ΔTc = 0.3 K) measurements.
本文言語 | English |
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ページ(範囲) | 33-37 |
ページ数 | 5 |
ジャーナル | Physica C: Superconductivity and its applications |
巻 | 378-381 |
号 | PART 1 |
DOI | |
出版ステータス | Published - 2002 10月 1 |
外部発表 | はい |
ASJC Scopus subject areas
- 電子材料、光学材料、および磁性材料
- 凝縮系物理学
- エネルギー工学および電力技術
- 電子工学および電気工学